Petisuix
Petisuix is the 300 MHz liquid spectrometer particularly opened to Phosphorus-31 experiments with its decoupled probe but which also accepts all heteronuclei! Temperature experiments are welcome.
This spectrometer is part of the ResoMag platform, the aim of which is to pool the various pieces of equipment from the laboratories belonging to the IP-Paris Department of Chemistry and Chemical Engineering.
The Bruker 300 MHz "Petal" NMR spectrometer is equipped with a 7 T magnet, a Bruker AvanceIII console and a TBO probe. The Petal spectrometer is primarily intended for routine use, with manual control using Topspin software. Its conditions of use are described in this short note, while its technical use is described in an operating manual available in the spectrometer room.
This spectrometer is primarily designed for 1H, 13C and 31P studies.
Outside routine periods, access to the spectrometer is via the simresa application (https://simresa.polytechnique.fr), at least 24 hours in advance.
Routine period (Monday to Friday from 9am to 11.30am and from 2pm to 7pm except Tuesday):
Experiment limited to 30 minutes per tube.
Booking period:
all experiments are authorized within the limits of the times and maximum duration defined in the table below. It must be done the day before at the latest. If no reservation is made, the spectrometer goes into "routine" mode.
booking period maximal duration of the booking remarks the week, 11.30am-2pm 2h30 Tuesdays, 9am-2pm 5hrs Nights, 7pm-9am 14hrs only 1 tube, more than one experiment on this tube weekends, from Friday 7pm to Monday 9am 62hrs only 1 tube, more than one experiment on this tube
