Agecanonix
The Bruker 400 MHz NMR spectrometer "Agecanonix" is equipped with a 9.4 T magnet, a Bruker AvanceI console and a BBO probe. The Agecanonix spectrometer has a 16-position changer of which only the first 9 are usable. It can be controlled by the ICON-NMR software. Agecanonix is mainly intended for routine use.
picture: Jérémy Barande - 2024
This spectrometer is part of the ResoMag platform, the aim of which is to pool the various pieces of equipment from the laboratories belonging to the IP-Paris Department of Chemistry and Processes.
The Bruker 400 MHz "Agecanonix" NMR spectrometer is equipped with a 9.4 T magnet, a Bruker AvanceI console and a BBO probe. The Agecanonix spectrometer has a 16-position changer, of which only the first 9 can be used. It can be controlled using ICON-NMR software. Agecanonix is primarily intended for routine use.
This spectrometer is mainly used for 1H and 13C studies, with the experiments summarised in the table below. The use of the autosampler is compulsory, whatever the period.
During the week (Monday to Friday), use of the ferry is divided into two periods. The times indicated are subject to change depending on the period, and in particular on the number of users. An information email will then be sent to you by the platform managers.
Day period (from Monday to Friday, between 9 am and 7.30pm):
Experiment limited to 15 minutes per tube.
Night time (7.30pm to 9am):
The tubes must be programmed and placed on the carousel from 5 p.m. or registered on the document next to the computer with the tubes placed in the pot provided. Only the experiments in the table below are authorised.
From Monday to Friday | |||||
Day (from 9am to 7.30pm) | Night (from 7.30pm to 9am) | ||||
Experience | duration | Experience | duration | ||
1H | 8 scans | 1 min 20 s | 1H | 8 scans | 1 min 20 s |
13C day | 64 scans | 2 min 40 s | 13C | 1024 scans | 41 min 32 s |
DEPT 135 | 256 scans | 14 min 46 s | |||
DEPT 90 | 256 scans | 14 min 46 s | |||
COSY | 9 min 02 s | ||||
HSQC | 14 min 11 s | ||||
HMBC | 30 min 31 s | ||||
Weekends (Friday 7.30pm to Monday 9am):
All experiments are authorised, particularly long characterisations (NOESY, low-concentration tubes, etc.), taking care not to exceed a total of 62 hours.
NB: The acquisition parameters can be modified by clicking on the 'Par' button for the number of scans (ns) and the lock and shims options. These options are left available, but experiments that are too long will not be accepted. Do not hesitate to discuss with a manager if your project requires a specific use (unstable products, etc.).