BobMorane

This spectrometer is part of the ResoMag platform, the aim of which is to pool the various pieces of equipment from the laboratories belonging to the IP-Paris Department of Chemistry and Processes.

The Bruker Bobmorane 300 MHz NMR spectrometer is equipped with a 7 T magnet, a Bruker AvanceII console and a BBFO probe. The Bobmorane spectrometer is primarily intended for routine use, with manual control using Topspin software. Its conditions of use are described in this short note, while its technical use is described in an operating manual available in the spectrometer room.

This spectrometer is primarily intended for studies of ¹H, ²⁹Si, ¹³C, ³¹P, ¹⁹F and all other heteronuclei.

Access to the spectrometer is via the simresa application (https://simresa.polytechnique.fr), no later than the previous day for a maximum of 24 hours. If you fail to make a reservation, Bobmorane will switch to "routine" mode. Weeknights (from 7pm to 9am) and weekends are by reservation only.

• Routine period (weekdays from 9am to 7pm):

• Experiment limited to 15 minutes per tube.

   

   

• Booking period:

• Day: from 9.00 am to 7.00 pm, must be made at the latest the day before

• Night: from 7pm to 9am. All experiments are permitted on a single tube, taking care not to exceed a total of 14 hours. It is possible to schedule several experiments on the same tube.

• Weekend: Friday 7pm to Monday 9am. All experiments are authorised on a single tube, taking care not to exceed the total of 62 hours. It is possible to schedule several experiments on the same tube.

• The timetable is subject to change due to public holidays during the week and priority events such as the Polytechnique entrance exam.

NB: Don't hesitate to talk to a manager if your project requires a specific use (unstable products, etc.).